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Class-leading with a proven track record,AutoPore Vsets a new standard for operational safety.
Capable of detecting pore sizes ranging from 3 nm to 1100 µm
High-resolution analysis is available for macroporous and mesoporous materials, allowing for severe quality control and providing full data for research, including intrusion and extrusion
Flexible reporting options can be configured to optimize the utility of the data collected
Enhancing operator safety is the top priority of recent enhancements
Multiple analysis modes are available for quick or extensive studies, emphasizing speed or resolution depending on the user’s needs
There are several configurations available to personalize the instrument based on user preferences, such as the number of analysis ports and operating pressure range
Ensures compliance with ASTM Test Methods D4284, D4404, and D6761, ISO 15901-1, and USP <267>
Description
Class Leading, Proven Performance
Mercury porosimetry analysis relies on the introduction of mercury into a porous material at carefully regulated pressures. Mercury porosimetry not only offers a wide measurement range, speed, and accuracy, but also makes it possible to calculate several sample attributes, such as sample densities (both bulk and skeletal), pore size distributions, total pore volume, total pore surface area, and median pore diameter.
Compared to other techniques, AutoPore V Series Mercury Porosimeters can assess a wider pore size distribution more quickly and accurately.
This device is outfitted with advanced safety measures. It includes new data reduction and reporting options, which provide further insights into the material’s pore shape and fluid transport properties.
Features and Benefits
Nineteen standard penetrometer sizes and combinations allow the investigation of a variety of sample sizes and forms
Provides rapid and thorough intrusion and extrusion analysis over a wide range of pore sizes
Sets a new standard in operator safety with the introduction of additional safety measures
Provides scanning and equilibration modes of operation for swift and comprehensive studies, respectively
Incorporates user-defined enhanced reporting features via Python scripts
Uses MicroActive software, enabling fast modifications to reporting ranges
Image Credit: Micromeritics Instrument Corporation
Technology
Operational Advantages
Capable of measuring pore sizes from 0.003 to 1100 µm (calculated with an initial filling pressure of 0.2 psia or 0.00128 MPa)
Controlled pressure can be gradually increased in precise increments of 0.05 psia, ranging from 0.2 to 50 psia, allowing thorough data collection in the macropore region
Operates in scanning mode and time- or rate-of-intrusion equilibrated modes
Real-time diagnostics provide information about possible problems before they become serious or affect the outcomes of analyses
Extraordinary precision is ensured by high-resolution (sub-microliter) measurement of intrusion/extrusion volumes, which makes it possible to develop tighter sample criteria, enhance manufacturing procedures, and provide high-quality research data
Improved linear motion for the high-pressure chamber’s closure
Gathers incredibly high-resolution data—it exceeds 0.1 µL for both the extrusion and mercury intrusion volumes
Design Advantages
Features four low-pressure and two high-pressure ports to help increase sample throughput
Enhanced safety features reduce the possibility of mercury leaks and operator exposure
Available in variants with pressure capacities of 33,000 and 60,000 psia
Quick-scan mode permits a continuous pressure rise, nearing equilibrium for faster screening
Features a low-noise and high-pressure producing system
Provides a variety of pressure ramping techniques, allowing selection of scanning mode for high-speed or on-demand results and equilibration mode for more exact and detailed results
Includes a temperature sensor for automatically estimating mercury density for penetrometer calibrations
MicroActive software allows for interactive data manipulation, unique report development, and rapid achievement of analytical findings
Provides a range of correction routines for baseline (automatic, differential, or manual), providing improved accuracy by mitigating compressibility and thermal effects caused by high-pressure
Compensates for material compression under high-pressure analysis
A New Benchmark for Operational Safety
Image Credit: Micromeritics Instrument Corporation
Specification
Source: Micromeritics Instrument Corporation
Electrical | |
---|---|
Voltage | 100/120/220/240 VAC ± 10 % |
Frequency | 50 or 60 Hz |
Power | 500 VA maximum |
Gas | |
Nitrogen or other clean, dry gas at 50 psig (345 kPa) | |
High-Pressure Model 9600 and 9605 | |
Measurement | From atmospheric pressure to 33,000 psia |
Resolution | 0.165 psia from 3,300 psia to 33,000 psia |
Transducer Accuracy | ±0 .1 % of full scale (transducer manufacturer’s specifications) |
Transducer Hysteresis | 0.05 % of full scale |
Pore Diameter Range | 6 to 0.005 μm |
Servo Control Precision | 0.5 % of target, min 5 psia, no overshoot |
High-Pressure Model 9610 and 9620 | |
Measurement | From atmospheric pressure to 60,000 psia |
Resolution | 0.03 psia from atmospheric pressure to 60,000 psia |
Transducer Accuracy | ± 0.1 % of full scale (transducer manufacturer’s specifications) |
Transducer Hysteresis | 0.05 % of full scale |
Pore Diameter Range | 6 to 0.003 μm |
Servo Control Precision | 0.5 % of target, min 5 psia, no overshoot |
Intrusion | |
Resolution | Better than 0.1 all |
Accuracy | ± 1 % of maximum penetrometer stem volume |
Low Pressure | All Models |
Measurement | 0.2 to 50 psia (345 kPa) |
Resolution | 0.00025 psi |
Pore Diameter Range | 1100 to 3.6 μm |
Transducer Accuracy | ± 1 % of full scale (transducer manufacturer’s specifications) |
Servo Control Precision | 1 % of target, min, 0.05 psia, no overshoot |
Penetrometers | |
Stem Intrusion Volumes | 0.38, 1.1, 1.7, 3.1, and 3.9 cc |
Sample Size | Maximum: a cylinder 2.54 cm diameter × 2.54 cm long (1 in. diameter × 1 in. long) |
Physical | |
Height | 143 cm (56.25 in.) |
Width | 54.3 cm (21.38 in.) |
Depth | 78 cm (30.75 in.) |
Weight | 250 kg (550 lb) |
Configuration
Four Models
The AutoPore V comes in four variants that are tailored to the unique needs of various quality assurance and research facilities.
Source: Micromeritics Instrument Corporation
9605 | 9620 | 9600 | 9610 | |
---|---|---|---|---|
Low Pressure | 4 ports | 4 ports | 2 ports | 2 ports |
High Pressure | 2 ports @ 33,000 psia | 2 ports @ 60,000 psia | 1 port @ 33,000 psia | 1 port @ 60,000 psia |
Penetrometers
Partial List
Source: Micromeritics Instrument Corporation
Model# | Size | Stem Volume | Medium | Typical Use |
---|---|---|---|---|
01 | 15 cc | 0.392 | Solid | refractories, low-porosity solid rocks/cores, low-porosity solid polymers |
02 | 15 cc | 0.392 | Powder | low-porosity powders, gravel, irregular rock shapes |
03 | 15 cc | 1.131 | Solid | medium-porosity rocks/cores, solid materials |
04 | 15 cc | 1.131 | Powder | medium-porosity rocks, solid materials, fumed silica |
07 | 5 cc | 0.392 | Solid | paper, flexible polymer/membrane sheets, pharma tablets |
08 | 5 cc | 0.392 | Powder | silicates, catalysts, powders (general use), pharma powders |
09 | 5 cc | 1.131 | Solid | medium/high-porosity sheet-form materials (paper, polymer, etc.), pharma tablets |
10 | 5 cc | 1.131 | Powder | silica-alumina, silicates, zeolites, catalysts, powders (general use), pharma powders |
14 | 3 cc | 0.412 | Powder | powders (general use), materials with low quantity available |
24 | 15 cc | 3.263 | Solid | high-porosity rock/cores, low-density/high-porosity foams |
25 | 15 cc | 4.185 | Solid | high-porosity material with large volume |
Accessories
Penetrometer Rack
Image Credit: Micromeritics Instrument Corporation
Penetrometers should be transported and stored securely to minimize damage and needless replacements.
Mercury QuikVac
Image Credit: Micromeritics Instrument Corporation
Mercury QuikVac provides an affordable way to handle mercury spills quickly. The instrument was specifically designed to collect minute mercury-contaminated particulate matter and elusive mercury droplets.
The recovered mercury is kept in a 250 mL recovery vessel, and the device discharges safe, clean air thanks to a replaceable 0.3–0.5 micron activated carbon filter.
Consumables and Supplies
Source: Micromeritics Instrument Corporation
Part Number | Description | Comments |
---|---|---|
950-61701-00 | Penetrometer Set, 15 cm3 Solid, 0.366 cm3 intrusion volume | Includes 1 each penetrometer 920-61701-01 and closure set 950-25832-00 |
950-61702-00 | Penetrometer Set, 15 cm3 Powder, 0.366 cm3 intrusion volume | Includes 1 each penetrometer 920-61702-01 and closure set 950-25832-00 |
950-61703-00 | Penetrometer Set, 15 cm3 Solid, 1.06 cm3 intrusion volume | Includes 1 each penetrometer 920-61703-01 and closure set 950-25832-00 |
950-61704-00 | Penetrometer Set, 15 cm3 Powder, 1.06 cm3 intrusion volume | Includes 1 each penetrometer 920-61704-01 and closure set 950-25832-00 |
950-61705-00 | Penetrometer Set, 15 cm3 Solid, 1.72 cm3 intrusion volume | Includes 1 each penetrometer 920-61705-01 and closure set 950-25832-00 |
950-61706-00 | Penetrometer Set, 15 cm3 Powder, 1.72 cm3 intrusion volume | Includes 1 each penetrometer 920-61706-01 and closure set 950-25832-00 |
950-61707-00 | Penetrometer Set, 5 cm3 Solid, 0.366 cm3 intrusion volume | Includes 1 each penetrometer 920-61707-01 and closure set 950-25831-00 |
950-61708-00 | Penetrometer Set, 5 cm3 Powder, 0.366 cm3 intrusion volume | Includes 1 each penetrometer 920-61708-01 and closure set 950-25831-00 |
950-61709-00 | Penetrometer Set, 5 cm3 Solid, 1.06 cm3 intrusion volume | Includes 1 each penetrometer 920-61709-01 and closure set 950-25831-00 |
950-61710-00 | Penetrometer Set, 5 cm3 Powder, 1.06 cm3 intrusion volume | Includes 1 each penetrometer 920-61710-01 and closure set 950-25831-00 |
950-61711-00 | Penetrometer Set, 5 cm3 Solid, 1.72 cm3 intrusion volume | Includes 1 each penetrometer 920-61711-01 and closure set 950-25831-00 |
950-61712-00 | Penetrometer Set, 5 cm3 Powder, 1.72 cm3 intrusion volume | Includes 1 each penetrometer 920-61712-01 and closure set 950-25831-00 |
950-61713-00 | Penetrometer Set, 3 cm3 Solid, 0.387 cm3 intrusion volume | Includes 1 each penetrometer 920-61713-01 and closure set 950-25831-00 |
950-61714-00 | Penetrometer Set, 3 cm3 Powder, 0.387 cm3 intrusion volume | Includes 1 each penetrometer 920-61714-01 and closure set 950-25831-00 |
950-61715-00 | Penetrometer Set, 3 cm3 Solid, 1.12 cm3 intrusion volume | Includes 1 each penetrometer 920-61715-01 and closure set 950-25831-00 |
950-61716-00 | Penetrometer Set, 3 cm3 Powder, 1.12 cm3 intrusion volume | Includes 1 each penetrometer 920-61716-01 and closure set 950-25831-00 |
950-61720-00 | Penetrometer Set, 3 cm3 Solid, 0.90 cm3 intrusion volume | Includes 1 each penetrometer 920-61720-01 and closure set 950-25831-00 |
950-61724-00 | Penetrometer Set, 15 cm3 Solid, 3.01 cm3 intrusion volume | Includes 1 each penetrometer 920-61724-01 and closure set 950-25832-00 |
950-61725-00 | Penetrometer Set, 15 cm3 Solid, 3.86 cm3 intrusion volume | Includes 1 each penetrometer 920-61725-01 and closure set 950-25832-00 |
920-61701-01 | Penetrometer, 15 cm3 Solid, 0.366 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61702-01 | Penetrometer, 15 cm3 Powder, 0.366 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61703-01 | Penetrometer, 15 cm3 Solid, 1.06 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61704-01 | Penetrometer, 15 cm3 Powder, 1.06 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61705-01 | Penetrometer, 15 cm3 Solid, 1.72 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61706-01 | Penetrometer, 15 cm3 Powder, 1.72 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61707-01 | Penetrometer, 5 cm3 Solid, 0.366 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61708-01 | Penetrometer, 5 cm3 Powder, 0.366 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61709-01 | Penetrometer, 5 cm3 Solid, 1.06 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61710-01 | Penetrometer, 5 cm3 Powder, 1.06 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61711-01 | Penetrometer, 5 cm3 Solid, 1.72 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61712-01 | Penetrometer, 5 cm3 Powder, 1.72 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61713-01 | Penetrometer, 3 cm3 Solid, 0.387 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61714-01 | Penetrometer, 3 cm3 Powder, 0.387 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61715-01 | Penetrometer, 3 cm3 Solid, 1.12 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61716-01 | Penetrometer, 3 cm3 Powder, 1.12 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61720-01 | Penetrometer, 3 cm3 Solid, 0.90 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25831-00 |
920-61724-01 | Penetrometer, 15 cm3 Solid, 3.01 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
920-61725-01 | Penetrometer, 15 cm3 Solid, 3.86 cm3 intrusion volume | Penetrometer glassware only; use with closure set 950-25832-00 |
950-33605-00 | Penetrometer Closure Kit for 3cm3 and 5 cm3 Penetrometers | Includes six 3 cm3 and 5 cm3 penetrometer closure sets, 950-25831-00, and closure nut holder 950-09802-00 and seal wrench 950-09803-00 |
950-33606-00 | Penetrometer Closure Kit for 15 cm3 Penetrometers | Includes six 15 cm3 penetrometer closure sets, 950-25832-00, and closure nut holder 950-09802-00 and seal wrench 950-09803-00 |
950-25831-00 | Closure Set for 3 cm3 and 5 cm3 Penetrometers | Includes 1 each closure nut 950-25831-01 and closure nut 950-25831-01 for 3 cm3 and 5 cm3 penetrometers |
950-25832-00 | Closure Set for 15 cm3 Penetrometers | Includes 1 each closure nut 950-25832-01 and closure nut 950-25832-01 for 15 cm3 penetrometers |
950-25831-01 | Closure Nut for 3 cm3 and 5 cm3 Penetrometers | Penetrometer closure nut for all 3 cm3 and 5 cm3 penetrometers |
950-25831-02 | Closure Seal for 3 cm3 and 5 cm3 Penetrometers | Penetrometer closure seal for all 3 cm3 and 5 cm3 penetrometers |
950-25832-01 | Closure Nut for 15 cm3 Penetrometers | Penetrometer closure nut for all 15 cm3 penetrometers |
950-25832-02 | Closure Seal for 15 cm3 Penetrometers | Penetrometer closure seal for all 15 cm3 penetrometers |
950-09802-00 | Penetrometer Closure Nut Holder | Used to hold penetrometer closure nut while tightening before analysis, and while loosening after analysis |
950-09803-00 | Penetrometer Closure Seal Wrench | Used to tighten penetrometer closure seal before analysis, and loosen seal after analysis |
950-25831-03 | Spacer for 3 cm3 and 5 cm3 Penetrometers | Used to properly position penetrometer while in low-pressure port to ensure connection to banana plug-in capacitance detector assembly |
942-25863-00 | Spacer for 15 cm3 Penetrometers | Used to properly position penetrometer while in low-pressure port to ensure connection to banana plug-in capacitance detector assembly |
962-25807-00 | Penetrometer Safety Enclosure | Holds penetrometer securely in place while viewing penetrometer installed into low-pressure port |
950-25822-00 | Penetrometer Weighing Support | Holds penetrometer assembly while weighing |
950-25820-00 | Rack for Penetrometer Storage | Securely holds empty penetrometers to help prevent breakage when not in use |
962-25827-00 | Rack for Filled Penetrometers | Holds filled penetrometers upright to facilitate movement between instrument and balance when determining Assembly Mass |
930-54601-00 | Cleaning Brush for Penetrometer with 0.4 cm3 Stem Volume | Used to clean inside 0.4 cm3 penetrometer stems |
930-54602-00 | Cleaning Brush for Penetrometer with 1.1 cm3 Stem Volume | Used to clean inside 1.1 cm3 penetrometer stems |
930-54603-00 | Cleaning Brush for Penetrometer with 1.8 cm3, 3.3 cm3, and 4.2 cm3 Stem Volume | Used to clean inside 1.8 cm3, 3.3 cm3, and 4.2 cm3 penetrometer stems |
Routine Operating Supplies | ||
004-16007-00 | Apiezon Type H High Vacuum Grease | Used to seal between penetrometer and closure nut |
920-16001-00 | High-Pressure Fluid, 1 L | Used to fill high-pressure chamber during analysis; not used in the hydraulic pump |
008-16045-00 | Silicone High Vacuum Grease | Used to lubricate low-pressure seals; apply small amount to penetrometer stems or low-pressure filler rods |
004-16011-00 | Hydraulic Pump Oil, Synthetic 15W-50 Grade | Used in the hydraulic pump that generates pressure for the high-pressure system; not used in the high-pressure port |
004-16004-01 | Triple Distilled Mercury | Ships as hazardous material; importation is limited by some countries. Check with Micromeritics' Representative for more details. |
942-25823-00 | Syringe, 50 mL |
For adding high-pressure fluid to the chamber, and for removing it from the chamber |
962-33601-00 | Operating Supplies | Includes one Liter of high-pressure fluid 920-16001-00, two unmodified banana plugs 003-21273-00, four modified banana plugs 930-25849-00, valve spanner 004-54039-00, mercury vapor filter 962-27000-00, and a package of 10 mercury vapor detection tubes |
962-33602-00 | Extended Operating Supplies | Includes Apiezon vacuum grease 004-16007-00, two Liters of high pressure fluid 920-16001-00, four unmodified banana plugs 003-21273-00, ten modified banana plugs 930-25849-00, valve spanner 004-54039-00, three mercury vapor filters 962-27000-00, and package of 10 mercury vapor detection tubes 962-29601-00 |
Routine Maintenance Supplies | ||
003-21273-00 | Banana Plug for Capacitance Detector Assemblies, unmodified | Replacement banana plugs for low-pressure and high-pressure capacitance detector assemblies |
922-09808-00 | Banana Plug Tool | For removal and replacement of banana plugs for capacitance detector assemblies and high-pressure feedthrough assemblies |
920-33616-00 | High-Pressure Vessel Maintenance Kit | Includes two each backup rings 004-25297-00, high-pressure seals 922-25890-00, O-rings for vent valve 004-25034-00, and modified banana plugs 930-25849-00, as well as six penetrometer contacts 930-25817-00 and instruction sheet |
922-33607-00 | High-Pressure Chamber Plug Seal Kit | Includes two each backup rings 004-25297-00 and high-pressure seals 922-25890-00, as well as an instruction sheet |
004-25297-00 | Backup Ring for High-Pressure Chamber Plug Seal | Replacement high-pressure chamber plug seal backup ring |
922-25890-00 | High-Pressure Chamber Plug Seal | Replacement high-pressure chamber plug seal |
004-25034-00 | O-ring for High-Pressure Chamber Vent Valve | Replacement O-ring for vent valve located on top of the high-pressure chamber |
930-25817-00 | Penetrometer contact for High-Pressure Chamber | Replacement penetrometer contact for high-pressure chamber plug |
930-25849-00 | Banana Plug for High-Pressure Feedthrough Assemblies, modified | Replacement banana plugs for high-pressure feedthrough assemblies in the bottom of the high-pressure ports |
962-33002-00 | Mercury Reservoir Cap Assembly | Replacement cap for mercury reservoir filling port |
004-25652-00 | O-ring for Mercury Reservoir Cap | Replacement O-ring for mercury reservoir filling port |
942-25600-00 | Cover for Spilled Mercury Containment Dish | Replacement cover for mercury spill containment dish |
003-51123-00 | 6.25 Amp Fuse, 3AG Slo-Blo 250 VAC | Replacement fuse for 100 to 120-volt installations |
003-51134-01 | 5 Amp Fuse, 5x20 mm Slo-Blo 250 VAC CE | Replacement fuse for 220 to 240-volt installations |
003-63801-01 | Ethernet Cable | Replacement Ethernet cable for connection of AutoPore to controlling computer |
004-54039-00 | Spanner for Solenoid Valves | Spanner to facilitate replacement of solenoid valve plungers |
930-17801-00 | Penetrometer Simulator, 82 pF | Penetrometer simulator for use when verifying calibration of capacitance detector system, 82 pF |
930-17801-01 | Penetrometer Simulator, 150 pF | Penetrometer simulator for use when verifying calibration of capacitance detector system, 150 pF |
930-17801-05 | Penetrometer Simulator, 15 pF | Penetrometer simulator for use when verifying calibration of capacitance detector system, 15 pF |
Reference Material and Reference Volume Capsules for Operational Verification | ||
004-16822-00 | Reference Material for Total Pore Volume and Median Pore Diameter | Reference material for operational verification |
940-34801-00 | Mercury Reference Volume Kit | Includes two small capsule assemblies 940-34800-00, 2 large capsule assemblies 940-34800-01, 25 replacement O-rings 004-25646-00, one package each of 8 µm membranes 940-25600-00 and 3 µm membranes 940-25600-01, storage case and instruction manual |
940-34800-00 | Small Mercury Reference Capsule Assembly | Reference volume capsule assembly, nominal 0.24 mL capacity |
940-34800-01 | Large Mercury Reference Capsule Assembly | Reference volume capsule assembly, nominal 0.80 mL capacity |
940-14800-00 | Reference Capsule Retaining Clip | Replacement retaining clip for reference volume capsule assemblies |
004-25646-00 | Reference Capsule O-ring | Replacement O-ring for reference volume capsule assemblies |
940-25600-00 | Reference Capsule 8 µm Member, Package of 100 | Replacement 8 µm membrane for reference volume capsule assemblies |
940-25600-01 | Reference Capsule 3 µm Member, Package of 100 | Replacement 3 µm membrane for reference volume capsule assemblies |
Mercury Safety Accessories | ||
090-00000-00 | QuikVac Mercury Clean-up Accessory | Mercury spill vacuum and containment accessory, capable of holding up to 250 mL of recovered mercury, with replaceable activated charcoal filter |
942-33021-00 | Exhaust Fan Kit | Optional kit to pull fresh air across mercury reservoir and then exhaust it to the rear of the instrument; port on the rear of instrument needs to be ducted properly to room ventilation system that is capable of handling mercury vapors |
962-25859-00 | Mercury Vapor Filter Assembly | Replacement mercury vapor filter for vacuum pump exhaust |
962-29600-00 | Mercury Vapor Detection Pump | Replacement mercury vapor detection pump for testing environment for mercury vapors using disposable mercury vapor detection tubes |
962-29601-00 | Mercury Vapor Detection Tube, Package of 10 | Replacement mercury vapor detection tubes for use with mercury vapor detection pump |
004-32031-00 | Low-Pressure Mercury Drip Tray | Replacement low-pressure mercury drip tray |
Low-Pressure Vacuum System Replacement Items and Supplies | ||
062-62801-11 | Vacuum Pump, 100 to 120 VAC | Replacement vacuum pump for evacuation of low-pressure system, for 100 to 120 VAC installations |
062-25801-23 | Vacuum Pump, 220 to 240 VAC | Replacement vacuum pump for evacuation of low-pressure system, for 220 to 240 VAC installations |
004-27040-00 | Vacuum Pump Exhaust Filter | Replacement exhaust filter for low-pressure vacuum pump |
004-16003-01 | Vacuum Pump Oil, 1L | Vacuum oil for low-pressure vacuum pump |
004-25630-00 | Centering Ring NW 16 | Replacement centering ring for connection to vacuum pump exhaust port |
004-25509-00 | Clamp NW 10/16 | Replacement clamp for connection to vacuum pump exhaust port |
Gas Supply Accessories | ||
004-62200-58 | Gas Regulator, 2-stage 100 psig outlet, CGA 580 gas cylinder fitting | Regulator for compressed gas supply to low-pressure system |
230-02001-00 | Gas Inlet Line, 1/8 inch OD x 6 feet L | Gas inlet line for compressed gas supply to low-pressure system |
004-25549-00 | Reducing Union, 1/4 inch to 1/8 inch | Reducing union to connect gas inlet line 230-02001-00 to gas regulator 004-62200-58 |
004-33601-00 | Two-outlet Expansion Kit for Gas Regulator | Expansion kit to allow use of one gas cylinder for multiple instruments |
004-33602-00 | Pressure Relief Kit for Gas Regulator | Used to prevent over-pressurization of gas regulator outlet |
Software and Operator's Manual | ||
962-20800-00 | AutoPore V Software | Latest version of AutoPore V operating software |
962-42800-00 | AutoPore V Operator's Manual | Printed AutoPore Operator's Manual, with binder |
Applications
Pharmaceuticals
Porosity and surface area are important in the purification, processing, mixing, tableting, and packaging of drugs. These aspects can also affect a drug’s shelf life, dissolving rate, and bioavailability.
Ceramics
Pore area and porosity have an influence on greenware curing and bonding. This is critical for defining the strength, texture, appearance, and density of the finished products.
Adsorbents
Understanding pore area, total pore volume, and pore size distribution is critical for maintaining quality control in industrial adsorbents and designing separation procedures. An adsorbent's selectivity is heavily influenced by its porosity and surface area properties.
Catalyst
Catalysts’ active surface area and pore shape both impact production rates. By limiting the pore size, only molecules of certain sizes are allowed to enter and depart, resulting in a selective catalyst that primarily creates the desired product.
Aerospace
The weight and usefulness of heat shields and insulating materials are affected by their surface area and porosity.
Fuel Cells
Fuel cell electrodes must have carefully controlled porosity and a large surface area to produce adequate power density.
Geoscience
Porosity is important in groundwater hydrology and petroleum exploration as it corresponds with the amount of liquid that a structure can contain and the effort required to retrieve it.
Filtration
Filter producers are interested in pore size, volume, shape, and tortuosity. Pore shape often has a greater direct influence on filtration than pore size since it is directly correlated with filtration performance and fouling.
Construction Materials
Diffusion, permeability, and capillary flow all have a substantial impact on the degradation process of concrete, cement, and other construction materials.
Paper
The porosity of the coating on print media is critical in offset printing, impacting aspects such as blistering, ink receptivity, and ink holdout.
Medical Implants
The weight and practicality of heat shields and insulating materials are affected by their surface area and porosity.
Software
Microactive for Autopore
Image Credit: Micromeritics Instrument Corporation
Intelligent, Intuitive, Interactive
MicroActive software significantly enhances functionality, ease of use, diagnostics, and data interpretation, establishing a new standard for high-performance mercury porosimetry.
Method Wizard
Create a method with an interactive step-by-step script, which simplifies the method development process and introduces new users to the AutoPore V.
Mercury Density Calculation
Unlike competing systems, which depend exclusively on mercury density at ambient temperature, the AutoPore V automatically detects the actual mercury temperature, providing accurate density calculations under operating circumstances.
User-Defined Reports and Report Options
Python scripting allows users to quickly build personalized advanced reports to meet particular needs. The new reporting options also provide automated report conversion to PDF or spreadsheet formats.
Post-Analysis Parameter Change
Post-analysis adjustments or corrections can be made to the analysis parameters (such as stem volume, maximum head pressure, and pen constant), reducing the need to rerun samples due to inaccuracies.
Reverberi Method Data Reduction
Obtain data on the distribution of pore shapes. This approach generates a three-dimensional array that depicts cavity and throat size in relation to volume.
Diagnostic Dashboard
Image Credit: Micromeritics Instrument Corporation
Real-time monitoring of critical system components enables proactive maintenance and troubleshooting.
Enhanced Penetrometer Calibration
Image Credit: Micromeritics Instrument Corporation
Makes automated volumetric or gravimetric calculations for penetrometer calibration easier.
Overlay Multiple Runs and Gas Adsorption Data
MicroActive for AutoPore V can overlay up to 25 runs and allows users to import pore size distributions from gas adsorption isotherms. This enables data analyzed from the micro to macropore range to be displayed in a single report.
Intelligent Data Reporting
When questionabledata is gathered, automatic alerts are issued.
Variety of Available Plots
Image Credit: Micromeritics Instrument Corporation
Users can view plots of pore volume, pore area, and pore size, as well as determine total intrusion volume, total pore (surface) area, average and median pore diameters, bulk or envelope density, and apparent (skeletal) density.
Reports Include:
Summary
Tabular Report
Cumulative Volume vs Pore Size/Particle Size/Pressure
Incremental Volume vs Pore Size/Particle Size/Pressure
Cumulative Area vs Pore Size/Particle Size/Pressure
Incremental Volume vs Pore Size/Particle Size/Pressure
Differential Reference % Volume vs Pore Size/Particle Size/Pressure
Out Spec. % Volume vs Pore Size/Particle Size/Pressure
Differential Volume vs Pore Size/Particle Size/Pressure
Cumulative Volume vs Pore Size/Particle Size/Pressure
Tortuosity
Permeability
Reverberi
Advanced Report System
Log Difference Volume vs Size
Material Compressibility
Cavity to Throat Size Ratio
Fractal Dimension
Mayer-Stowe Particle Size
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